You should have:

• Purpose
• Name, Structure, Physical properties, and Hazards of ALL chemicals
  • Physical properties: MW, mp/bp, density, color, solubility in water
  • Hazards: NFPA codes, LD50, precautions beyond goggles and lab coat (if applicable)
• Procedure (left side of page, past tense)
• Drawings of an unusual, complicated, or new apparatus
• Observations (right side) of
  • starting materials, crude products, purified products
  • colors, state changes, etc… during reaction
  • masses (starting materials, crude products, purified products etc…)
  • characterization observations (mp/bp)
  • Also any alterations to the procedure
• Drawings of TLC plates (to scale, indicate spot colors, indicate visualization method)
• Results and calculation section
  • Summary of characterization data:
    • Experimental mp/bp values
      • Also list literature values of starting materials, desired products, and any likely side products for comparison
    • Major peak values and characteristic (broad/sharp strong/weak) from IR with functional group assignments
    • Peak shifts, splitting and integration values from ¹H NMR
      • Assign these peaks to the expected product molecule or to common NMR impurities from the bookmark in CC (MUST CITE impurity assignments)
        • Impurities may be water, acetone, CHCl₃ if using CDCl₃, dimethylsulfoxide (DMSO) if using D₆DMSO
  • Calculations
    • Percent yield (actual yield / theoretical yield * 100%)
    • Atom Economy (MW desired product / S MW starting materials * 100%)
    • Effective Mass Yield (EMY) (mass product / mass hazardous reagents * 100%)
      • Must indicate how you define “hazardous”
    • E-Factor (mass total waste / mass product)
• Conclusions
  • For EACH STEP make a conclusion if the reaction was successful
    • What evidence supports that you created the desired product?
      • Be specific, use ALL of your characterization data
      • State if there is any conflicting characterization data
    • Was your reaction efficient?
      • Use % yield, and Atom Economy
    • Was your product pure?
      • If the characterization data suggests there is impurities, is it easy to remove solvent, or is there evidence of some side product that may be harder to remove?

– Attached is the experiment file.